HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Nitro-2-propoxyaniline → 2,4-Diaminopropoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Nitro-2-propoxyaniline | HCID 11118 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2,4-Diaminopropoxybenzene | HCID 153693 | — |
Reaction Steps
4-Propoxybenzene-1,3-diamine (D-5) was synthesized following the general scheme above starting from 5-nitro-2-propoxy-phenylamine. Yield (79%). HPLC ret. time 0.54 min, 10-99% CH3CN, 5 min run; ESI-MS 167.5 m/z (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802700B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-a685ae86a57c4735836b6b8c1bb7917e |
| Source note | uspto-grants-2014_08 |