HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbenzeneethanol → 4-Nitro-3-(2-m-tolyl-ethoxy)-benzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbenzeneethanol | HCID 74648 | — |
| Reactant | Methyl 3-hydroxy-4-nitrobenzoate | HCID 294866 | — |
| Product | 4-Nitro-3-(2-m-tolyl-ethoxy)-benzoic acid methyl ester | HCID 67076436 | 86.9% |
Reaction Steps
3-Hydroxy-4-nitro-benzoic acid methyl ester (1.00 g, 5.07 mmol) and 2-(3-methylphenyl)-ethanol (0.829 g, 6.09 mmol) were reacted in analogy to step 1 of example 1 to give 1.39 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802720B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-245f82be1c0044ecaeff642b3d0cb5e6 |
| Source note | uspto-grants-2014_08 |