HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3,3-Triethoxyprop-1-yne → 3-Ethoxy-5-triethoxyprop-1-ynyl-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3,3-Triethoxyprop-1-yne | HCID 10920972 | — |
| Reactant | 3-Bromo-5-ethoxypyridine | HCID 12293480 | — |
| Product | 3-Ethoxy-5-triethoxyprop-1-ynyl-pyridine | HCID 22570255 | 37% |
Reaction Steps
The title compound was synthesized from 3-bromo-5-ethoxy-pyridine and 3,3,3-triethoxypropyne using the procedure described in Example 43, step (e), in 37% yield. 1H NMR (CDCl3) δ 8.27 (bs, 1H), 8.24 (bs, 1H), 7.21 (m, 1H), 4.02 (q, 2H, J=7.0 Hz), 3.72 (q, 6H, J=7.0 Hz), 1.39 (t, 3H, J=7.0 Hz), 1.23 (t, 9H, J=7.0 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06855722B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-cc717a44db274c4f95c9de13457091b9 |
| Source note | uspto-grants-2005_02 |