2,4-Dichlorobenzaldehyde → HCID 24960743, compound

HRID 2405543Notes

Reaction equation

HRID 2405543 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:18])[CH2:9][S:10][C:11]2[CH:16]=[CH:15][C:14]([Br:17])=[CH:13][CH:12]=2)=[CH:4][CH:3]=1.[Cl:19][C:20]1[CH:27]=[C:26]([Cl:28])[CH:25]=[CH:24][C:21]=1[CH:22]=O>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8](=[O:18])/[C:9](/[S:10][C:11]2[CH:16]=[CH:15][C:14]([Br:17])=[CH:13][CH:12]=2)=[CH:22]\[C:21]2[CH:24]=[CH:25][C:26]([Cl:28])=[CH:27][C:20]=2[Cl:19])=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 134042,4-DichlorobenzaldehydeHCID 43412626HCID 43412626, compound

Product 1

HCID 24960743HCID 24960743, compound

Procedure

The title compound is prepared by the methods described in Synthesis Example 1. A solution of 1-(4-bromophenyl)-2-(4-bromophenylthio)ethanone (10 mmol) and 2,4-dichlorobenzaldehyde (10 mmol) was subjected to the procedure described as Method B in part C of Synthesis Example 1 and the product obtained was purified by column chromatography.

Workup

  1. customdescribed in Synthesis Example 1
  2. customdescribed as Method B in part C of Synthesis Example 1
  3. customthe product obtained
  4. customwas purified by column chromatography

Sources & evidence

ORD record
ord-fab33517ad5e4f3691f8b0722ef5341f
Source dataset
uspto-grants-2014_08
Patent number
US08808702B2

Reaction notes

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