HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 240566Generated: October 26, 2026
2-Amino-5-nitrobenzoic acid → HCID 178526470, compound
https://huagongshe.com/reaction/240566
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Amino-5-nitrobenzoic acid | HCID 12032 | — |
| Reactant | Formamidine acetate | HCID 160693 | — |
| Solvent | 1-Methoxyethanol | HCID 3015637 | — |
| Product | HCID 178526470 | HCID 178526470 | — |
Reaction Steps
A mixture of 2-amino-5-nitrobenzoic acid (1000 g, 5 mol) and formamidine acetate (1000 g, 10 mol) were dissolved in methoxyethanol (4 L) and heated to 115° C. for 16 hours. After cooling the mixture to room temperature, ice water (5 L) was added and the mixture was stirred for 30 minutes before collecting the product (125 g, 14%) by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08648087B2 |
|---|
| Source dataset | uspto-grants-2014_02 |
|---|
| ORD ID | ord-c6eaa425e0df4e24ab878d970d8aa4c3 |
|---|
| Source note | uspto-grants-2014_02 |
|---|
