HRID240574

反应详情

EQUATION

反应方程式

HRID 240574 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 2-nitrobenzene-1,4-diol (3.00 g, 19.34 mmol) in ethanol (100 mL) was added 10% palladium on carbon (0.600 g, 0.564 mmol). After shaking under 40 psi of hydrogen for 2 hours, the mixture was filtered and the filtrated was concentrated under reduced pressure to provide the product as solid.

WORKUP

后处理

  1. filtrationthe mixture was filtered
  2. concentrationthe filtrated was concentrated under reduced pressure