Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | 6-Amino-1,2-dihydroisoquinolin-1-one | HCID 51342001 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 24863360 | HCID 24863360 | — |
Reaction Steps
6-Amino-2H-isoquinolin-1-one (0.2 mmol, 39 mg) and benzyl isocyanate (0.2 mmol, 27 mg) were dissolved in 1 mL DMA. The mixture was allowed to stir at 60° C. overnight. The product was obtained by HPLC purification. MS (M+1) 294.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08809326B2 |
|---|
| Source dataset | uspto-grants-2014_08 |
|---|
| ORD ID | ord-6af916e923b44959990e43cbc3e1ffba |
|---|
| Source note | uspto-grants-2014_08 |
|---|
