HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Difluoroethan-1-ol → 2,2-Difluoroethyl sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Difluoroethan-1-ol | HCID 136187 | — |
| Reactant | Cyclopropyl sulfamate | HCID 57785190 | — |
| Product | 2,2-Difluoroethyl sulfamate | HCID 57785155 | — |
| Product | N-(2,2-difluoroethyl)sulfamate | HCID 86632791 | — |
Reaction Steps
2,2-Difluoroethylsulfamate was synthesized according to the method presented in the synthesis of sulfamic acid cyclopropyl ester in Example 1 with the exception of utilizing 2,2-difluoroethylalcohol to obtain sulfamic acid 2,2-difluoro-ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809267B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-64215ffef70a4f14a90ef06a69107557 |
| Source note | uspto-grants-2014_08 |