Phenylsulfamate → Sulfamic acid 1-isopropyl-cyclopropyl ester
反応式
[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=[CH:5]C=[CH:3][CH:2]=1.[CH:12](C1(O)CC1)(C)C>>[CH:6]([C:1]1([O:7][S:8](=[O:10])(=[O:11])[NH2:9])[CH2:2][CH2:3]1)([CH3:5])[CH3:12]参加物
3
実験手順
Sulfamic acid 1-isopropyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-isopropylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234) to obtain sulfamic acid 1-isopropyl-cyclopropyl ester.
後処理
- customSulfamic acid 1-isopropyl-cyclopropyl ester was synthesized
出典と根拠
- ORDレコード
- ord-62687145003943148b17ee20b9fdd5f2
- 出典データセット
- uspto-grants-2014_08
- 特許番号
- US08809267B2
反応ノート
読み込み中…