Phenylsulfamate → HCID 57785565, compound

HRID 2405796Notes

Reaction equation

HRID 2405796 reaction equation
[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=CC=[CH:3][CH:2]=1.[CH3:12][O:13]CC1(O)CC1>>[CH3:12][O:13][CH2:6][C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 11030308PhenylsulfamateHCID 574451551098183-67-5

Product 1

HCID 57785565HCID 57785565, compound

Procedure

Sulfamic acid 1-methoxymethyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-methoxymethyl cyclopropanol (synthesized by methods reported in European Journal of Chemistry 2006, 5069) to obtain sulfamic acid 1-methoxymethyl-cyclopropyl ester.

Workup

  1. customSulfamic acid 1-methoxymethyl-cyclopropyl ester was synthesized

Sources & evidence

ORD record
ord-91f2572ea14a45a185326ea49d1c4e6b
Source dataset
uspto-grants-2014_08
Patent number
US08809267B2

Reaction notes

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