Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57704526 | HCID 57704526 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67418521 | HCID 67418521 | — |
Reaction Steps
Compound 28-5 (500 mg) was dissolved in ethanol (15 ml), concentrated hydrochloric acid (1.5 ml) was added, and the mixture was stirred at 80° C. for 1.5 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (330 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08809304B2 |
|---|
| Source dataset | uspto-grants-2014_08 |
|---|
| ORD ID | ord-9369fe749c284fe0ab2f0c7810bbec21 |
|---|
| Source note | uspto-grants-2014_08 |
|---|
