2-Hex-1-enyl-1H-indole → HCID 14299246, compound

HRID 2406628Notes

Reaction equation

HRID 2406628 reaction equation
[CH:1]([C:7]1[NH:8][C:9]2[C:14]([CH:15]=1)=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:2][CH2:3][CH2:4][CH2:5][CH3:6]>C(O)C.[Pd]>[CH2:1]([C:7]1[NH:8][C:9]2[C:14]([CH:15]=1)=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

4

Reactant 1

HCID 666441492-Hex-1-enyl-1H-indole

Product 1

HCID 14299246HCID 14299246, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

2-Hex-1-enyl-1H-indole was dissolved in ethanol and 10% palladium on carbon was added to the solution. The reaction flask was sealed and exposed to hydrogen gas under pressure until the hydrogen gas consumption was stopped completely. The reaction mixture was filtered through Celite. The solvent was evaporated to afford the product.

Workup

  1. customThe reaction flask was sealed
  2. customexposed to hydrogen gas under pressure until the hydrogen gas consumption
  3. filtrationThe reaction mixture was filtered through Celite
  4. customThe solvent was evaporated
  5. customto afford the product

Sources & evidence

ORD record
ord-5ef354922c5a4edf996e8a5ab0f148e7
Source dataset
uspto-grants-2014_08
Patent number
US08809382B2

Reaction notes

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