HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 49802316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 66644066 | HCID 66644066 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 49802316 | HCID 49802316 | — |
Reaction Steps
To the cold solution of 5-(6-Chloro-2-hexyl-indol-1-yl)-3-(S)-methyl-5-oxo-pentanoic acid 2-trimethylsilanyl-ethyl ester in methylene chloride was added trifluoro acetic acid and was stirred for three days. The reaction mixture was then treated with water and ethyl acetate. The product was purified by column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809382B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-3e3cef763ae74d3fba95dc7e04f163a9 |
| Source note | uspto-grants-2014_08 |