HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68613896, compound → 2-Methoxy-7-quinolinamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68613896 | HCID 68613896 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Methoxy-7-quinolinamine | HCID 68614312 | 99.5% |
Reaction Steps
A methanol (10 ml) solution containing 2-methoxy-7-nitroquinoline (33 mg) obtained in the 1st step was prepared and subjected to a hydrogenation reaction (60° C.; 50 bar; flow rate: 1 ml/min; 10% Pd/C) using H-cube™. Then, the solvent was distilled away under reduced pressure, and a purple solid of 2-methoxyquinolin-7-amine (28 mg) was thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809371B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-300ad33cc96842d7b1b05e7c8c479cb5 |
| Source note | uspto-grants-2014_08 |