HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-N-phenyl-hydrazine → 5-(4-chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid N'-methyl-N'-phenyl-hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| Reactant | 5-(4-Chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-nicotinic acid | HCID 66686971 | — |
| Product | 5-(4-chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid N'-methyl-N'-phenyl-hydrazide | HCID 71294427 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 1 using 5-(4-chlorophenyl)-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid (CAN 1018782-82-5) and 1-methyl-1-phenyl-hydrazine (CAN 618-40-6) as starting materials; MS (EI) 436.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648099B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-7c8b2c96f5f84582ab96174c654b13c2 |
| Source note | uspto-grants-2014_02 |