HCID 131731780, compound → 2-(Acetoacetoxy)ethyl methacrylate

HRID 2406906Notes

Reaction equation

HRID 2406906 reaction equation
COC(=O)C(C)=C.C(OCCCC)(=O)C=C.C(O)(=O)C=C.[CH3:22][C:23]([C:25]([O:27][CH2:28][CH2:29][O:30][C:31]([CH2:33][C:34]([CH3:36])=[O:35])=[O:32])=[O:26])=[CH2:24]>O>[CH3:24][C:23]([C:25]([O:27][CH2:28][CH2:29][O:30][C:31]([CH2:33][C:34]([CH3:36])=[O:35])=[O:32])=[O:26])=[CH2:22]

Participants

3

Reactant 1

HCID 131731780HCID 131731780, compound

Product 1

HCID 888552-(Acetoacetoxy)ethyl methacrylate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Same procedure as Example 8 except monomers pre-emulsion was prepared by mixing 135 g of water, 7 g of Dowfax 2A1 surfactant and 300 g of acrylic monomers consisting of methylmethacrylate/n-butyl acrylate/acrylic acid/AAEM in ratio of 40.0/48.0/2.0/10.0. Resulting latex had the following properties:

Workup

  1. customSame procedure as Example 8 except monomers pre-emulsion was prepared
  2. customResulting latex

Sources & evidence

ORD record
ord-8ec814ab89f947a89e6bb88c8f858996
Source dataset
uspto-grants-2014_08
Patent number
US08809446B2

Reaction notes

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