HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyl iodide → HCID 66780718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyl iodide | HCID 85247 | — |
| Reactant | HCID 11326794 | HCID 11326794 | — |
| Reactant | HCID 66781128 | HCID 66781128 | — |
| Product | HCID 66780718 | HCID 66780718 | 34% |
Reaction Steps
This compound was prepared as described for 3f, using 21 (154 mg, 0.41 mmol) as a starting material and iodotrimethysilane (0.47 mL, 3.3 mmol). Compound 3g (50 mg, 0.14 mmol) was obtained as a colorless solid, in 34% yield, which was characterized as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809520B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fdc5eee9232f4231879b3faa17a06c26 |
| Source note | uspto-grants-2014_08 |