HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-(3-Methoxyphenyl)-1,2,4-triazin-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 67363595 | HCID 67363595 | — |
| Product | 5-(3-Methoxyphenyl)-1,2,4-triazin-3-amine | HCID 7176086 | 45% |
Reaction Steps
5-(3-Methoxyphenyl)-1,2,4-triazin-3-amine (0.31 g, 45%) was prepared from 3-(methylsulfonyl)-5-(3-methoxyphenyl)-1,2,4-triazine (0.90 g, 3.39 mmol) and 0.5 M ammonia in THF (50 mL, 25.0 mmol) according to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809525B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-77481477eb6940c5bd27c34028138ef4 |
| Source note | uspto-grants-2014_08 |