HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 67362885, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 67365040 | HCID 67365040 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67362885 | HCID 67362885 | 85% |
Reaction Steps
5-[4-(methoxymethyl)phenyl]-1,2,4-triazin-3-amine (2.2 g, 85%) was prepared from 5-[4-(methoxymethyl)phenyl]-3-(methylsulfonyl)-1,2,4-triazine (3.40 g, 12.2 mmol) in THF (35 mL) and treated with NH3 gas by purging for 30 minutes, similarly to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809525B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-8b97e16f8c504cde81a4bba30087c84c |
| Source note | uspto-grants-2014_08 |