HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86676113, compound → 3-(Methylsulfanyl)-5-(3-chloro-5-fluorophenyl)-1,2,4-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86676113 | HCID 86676113 | — |
| Reactant | Methyl hydrazinecarbimidothioate | HCID 178504051 | — |
| Product | 3-(Methylsulfanyl)-5-(3-chloro-5-fluorophenyl)-1,2,4-triazine | HCID 67365706 | 38.6% |
Reaction Steps
3-(methylsulfanyl)-5-(3-chloro-5-fluorophenyl)-1,2,4-triazine (16 g, 38.4%) was prepared from methyl hydrazinecarbimidothioate (25.5 g, 243 mmol) and 2-(3-chloro-5-fluorophenyl)-2-oxoacetaldehyde (30 g, 162 mmol) according to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809525B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-e54a49346d0a4cab917ec2a6aa989e86 |
| Source note | uspto-grants-2014_08 |