反应详情

温度

150 °C

Phenylethynyltri-n-butyltin (8.25 g, 21.1 mmol) and benzyl azide (2.3 mL, 18.4 mmol) were combined and heated to 150° C. overnight. The mixture was purified by silica gel chromatography eluting with a gradient of 5-40% ethyl acetate in hexanes to afford the title compound. MS (ESI+) m/z 526.3 (M+H)+.

1. customThe mixture was purified by silica gel chromatography
2. washeluting with a gradient of 5-40% ethyl acetate in hexanes