HCID 11298722, compound → HCID 58504231, compound

HRID 2407693Notes

Reaction equation

HRID 2407693 reaction equation
Cl.[C:2]1([C:8]2[C:12]3=[C:13]([NH:17][CH2:18][CH:19]4[CH2:24][CH2:23][NH:22][CH2:21][CH2:20]4)[N:14]=[N:15][CH:16]=[C:11]3[O:10][N:9]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[C:32]1[CH:36]=[C:35]([CH:37]=O)[O:34][N:33]=1>>[Cl:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[C:32]1[CH:36]=[C:35]([CH2:37][N:22]2[CH2:23][CH2:24][CH:19]([CH2:18][NH:17][C:13]3[N:14]=[N:15][CH:16]=[C:11]4[O:10][N:9]=[C:8]([C:2]5[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=5)[C:12]=34)[CH2:20][CH2:21]2)[O:34][N:33]=1

Participants

3

Reactant 2

HCID 11298722HCID 11298722, compoundHCID 66989956HCID 66989956, compound

Product 1

HCID 58504231HCID 58504231, compound

Procedure

According to the same procedure described in Example 35, using the compound obtained in Example 84 instead of the compound obtained in Example 11 and 3-(2-chlorophenyl)isoxazole-5-carbaldehyde instead of 4-phenylthiophene-2-carbaldehyde, the title compound having the following physical data was obtained.

Sources & evidence

ORD record
ord-bb071826edf648b0988b33cfe2e03966
Source dataset
uspto-grants-2014_08
Patent number
US08809538B2

Reaction notes

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