HCID 11298722, compound → HCID 58504054, compound
Reaction equation
[C:1]1([C:7]2[C:11]3[C:12]([O:16][CH2:17][CH:18]4[CH2:23][CH2:22][NH:21][CH2:20][CH2:19]4)=[N:13][N:14]=[CH:15][C:10]=3[O:9][N:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[C:31]1[CH:35]=[C:34]([CH:36]=O)[O:33][N:32]=1>>[Cl:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[C:31]1[CH:35]=[C:34]([CH2:36][N:21]2[CH2:22][CH2:23][CH:18]([CH2:17][O:16][C:12]3[C:11]4[C:7]([C:1]5[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=5)=[N:8][O:9][C:10]=4[CH:15]=[N:14][N:13]=3)[CH2:19][CH2:20]2)[O:33][N:32]=1Participants
3
Procedure
According to the same procedure described in Example 35, using the compound obtained in Example 89 instead of the compound obtained in Example 11 and 3-(2-chlorophenyl)isoxazole-5-carbaldehyde instead of 4-phenylthiophene-2-carbaldehyde, the title compound having the following physical data was obtained.
Sources & evidence
- ORD record
- ord-02150eaa6f4645f3ad6edbce8a231556
- Source dataset
- uspto-grants-2014_08
- Patent number
- US08809538B2
Reaction notes
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