N-bromobutanimide → HCID 58504032, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of the compound prepared in Example 151 (3.50 g) and N-bromosuccinimide (2.66 g) and benzoyl peroxide (0.362 g) in carbon tetrachloride (80 mL) was heated at 90° C. for 18 hours. The mixture was partitioned between a saturated aqueous sodium bicarbonate solution and dichloromethane. The organic layer was dried over anhydrous magnesium sulfate and concentrated to obtain the title compound (4.70 g) having the following physical data.

Provenance & Evidence