Potassium Sodium Tartrate → HCID 58504027, compound

Participants

Reaction Steps

The compound prepared in Example 153 (180 mg) in tetrahydrofuran (2 mL) was stirred at 0° C. for 30 minutes. Lithium aluminum hydride (1.30 g) was added and the reaction was stirred for 18 hours. Rochelle's salt (sodium potassium tartrate; 10 g) was added and the solution was stirred for 30 minutes. The mixture was then partitioned between a saturated aqueous sodium bicarbonate solution and ethyl acetate. The organic layer was dried over anhydrous magnesium sulfate and concentrated to obtain the title compound (0.096 g) having the following physical data.

Provenance & Evidence