HCID 58504068, compound → HCID 58504081, compound

Participants

Reaction Steps

The compound prepared in Example 301 (1.30 g) was suspended in ethyl acetate (4.0 mL) and platinum (IV) oxide (81.9 mg, 0.361 mmol) added. The reaction mixture was stirred at room temperature under a balloon of hydrogen for 18 hours and then concentrated under reduced pressure to afford the crude material, which was purified by flash column chromatography (eluant: 10% ethyl acetate/hexane) to furnish the title compound (1.00 g) with the following physical properties.

Provenance & Evidence