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HRID2407935

反应详情

EQUATION

反应方程式

HRID 2407935 的结构方程式

REACTANTS

反应物

1
结构：CCOP(=O)(CCOCCOCCOC[C@H](C)NC(=O)OC(C)(C)C)OCC
HCID86678314

未命名化合物

PRODUCTS

生成物

1
结构：CCOP(=O)(CCOCCOCCOC[C@H](C)N)OCC
HCID86678313

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

A solution of (S)-tert-butyl (1-(2-(2-(2-(diethoxyphosphoryl)ethoxy)ethoxy)ethoxy)propan-2-yl)carbamate (1 eq) in 4N HC1/dioxane (0.4 M) was stirred at 25° C. for 1 hour. The reaction mixture was concentrated en vaccuo to give the title product as a colorless viscous oil.

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated en vaccuo