huagongshe.com
HRID2407940

反应详情

EQUATION

反应方程式

HRID 2407940 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCCCCCCCOC[C@H](CSC[C@H](NC(=O)OCC1c2ccccc2-c2ccccc21)C(=O)O)NC(=O)CCCCCCCCCCC
HCID67402076

未命名化合物

结构：CCOP(=O)(CCOCCOCCNC(=O)[C@H](C)N)OCC
HCID86678315

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCOC[C@H](CSC[C@H](N)C(=O)N[C@@H](C)C(=O)NCCOCCOCCP(=O)(O)O)NC(=O)CCCCCCCCCCC
HCID53476781

未命名化合物

PROCEDURE

实验过程

The title product was prepared from (R)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(((R)-2-dodecanamido-3-(dodecyloxy)propyl)thio)propanoic acid (1 eq, from example 26, step 8) and (S)-diethyl (2-(2-(2-(2-aminopropoxy)ethoxy)ethoxy)ethyl)phosphonate (1.2 eq, from example 30, step 2) by following the procedure described for example 28, step 3-5. 1H NMR (DMSO-d6): δ 9.38 (br s, 1H), 8.14 (t, 2H), 4.18-4.25 (m, 1H), 3.92-4.00 (m, 1H), 3.06-3.67 (m, 15H), 2.92 (dd, 2H), 2.79 (dd, 2H), 2.59-2.73 (m, 4H), 2.07 (t, 2H), 1.65-1.75 (m, 2H), 1.42-1.50 (m, 4H), 1.21-1.28 (m, 35H), 0.85 (t, 6H). LRMS [M+H]=811.5.