tert-Octylamine → HCID 86656469, compound

HRID 240826Notes

Reaction equation

HRID 240826 reaction equation
[N:1]([CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[C:2]=[S:3].[C:11]([NH2:19])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]>>[C:11]([NH:19][C:2]([NH:1][CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[S:3])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]

Participants

3

Reactant 2

HCID 61017tert-OctylamineHCID 101763092-(2-Isothiocyanatoethyl)thiophene

Product 1

HCID 86656469HCID 86656469, compoundYield 83%

Procedure

The procedure of step (1-1) of Example 1 was repeated except for using the compound obtained in step (2-1) (2.5 g, 15.0 mmol) and t-octyl amine (1.6 mL, 10.2 mmol), to obtain the title compound (2.5 g, 83%).

Sources & evidence

ORD record
ord-c833821c4062406bbd394a19d3e2b44e
Source dataset
uspto-grants-2014_02
Patent number
US08648111B2

Reaction notes

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