Hexachlorocyclotriphosphazene → HCID 57730740, compound

Participants

Reaction Steps

500 mg of 4-hydroxybenzaldehyde sodium salt (3.47 mmol) is added at 0° C. and under an inert atmosphere to a solution containing 4.8 g of hexachlorocyclotriphosphazene (13.8 mmol) in THF (200 mL). The reaction medium is stirred for 12 hours while the temperature is left to gradually return to room temperature. The crude reaction product is evaporated to dryness then purified by “flash” chromatography on a silica column. The product is isolated in the form of a translucent oil with a yield of 75%.

Provenance & Evidence