HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromonitromethane → 5-(Tert-butyl)-2-nitroselenophene-3-ylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromonitromethane | HCID 68423 | — |
| Reactant | Sodium selenide | HCID 73973 | — |
| Reactant | 3-Chloro-4,4-dimethylpent-2-enenitrile | HCID 2735661 | — |
| Product | 5-(Tert-butyl)-2-nitroselenophene-3-ylamine | HCID 86698284 | — |
Reaction Steps
The reaction of 3-chloro-4,4-dimethylpent-2-enenitrile, sodium selenide and bromonitromethane as described earlier gave the product as a yellow color solid, mp 112-114° C. 1H NMR (400 MHz, DMSO-d6): δ 8.28 (2H, br s), 6.76 (1H, s), 1.28 (9H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815879B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-033231bcad7447bd8af9e20b9d42b2f1 |
| Source note | uspto-grants-2014_08 |