HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroaniline → HCID 71179045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroaniline | HCID 7240 | — |
| Reactant | HCID 178469627 | HCID 178469627 | — |
| Product | HCID 71179045 | HCID 71179045 | 31.4% |
Reaction Steps
Using ethyl 7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylate (3.00 g, 14.5 mmol) and 2-chloroaniline (2.77 g, 21.7 mmol) instead of 4-fluoro-2-methylaniline, and in the same manner as in Example 1 step 1, the title compound (1.44 g, 31%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-048351b626ff4918a84d0f6eaa074f52 |
| Source note | uspto-grants-2014_08 |