HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-p-toluidine → HCID 71178929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-p-toluidine | HCID 12007 | — |
| Reactant | HCID 178469627 | HCID 178469627 | — |
| Product | HCID 71178929 | HCID 71178929 | 35% |
Reaction Steps
Using ethyl 7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylate (15.0 g, 72.4 mmol) and 2-chloro-4-methylaniline (20.5 g, 144.7 mmol) instead of 4-fluoro-2-methylaniline, and in the same manner as in Example 1 step 1, the title compound (8.37 g, 35%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-913a0dc06403417d971f03eb4a722dc7 |
| Source note | uspto-grants-2014_08 |