HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-3-oxetanecarboxylic Acid → HCID 71179085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-3-oxetanecarboxylic Acid | HCID 14028997 | — |
| Reactant | HCID 71178992 | HCID 71178992 | — |
| Product | HCID 71179085 | HCID 71179085 | 79.4% |
Reaction Steps
Using 7-(2,5-dichlorophenylamino)-6-[4-(4-fluorophenyl)piperidine-1-carbonyl]pyrazolo[1,5-a]pyrimidine-3-sulfonamide (0.07 g, 0.12 mmol) obtained in Example 22 step 5 and 3-methyloxetane-3-carboxylic acid (0.072 g, 0.62 mmol) instead of cyclopropanecarboxylic acid, and in the same manner as in Example 1 step 6, the title compound (0.063 g, 76%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-955b6c4664d34367a9502f51e789d8c0 |
| Source note | uspto-grants-2014_08 |