HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-5-methylaniline → HCID 71178910, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-5-methylaniline | HCID 262970 | — |
| Reactant | HCID 178469627 | HCID 178469627 | — |
| Product | HCID 71178910 | HCID 71178910 | 62.6% |
Reaction Steps
Using ethyl 7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylate (5.0 g, 24.1 mmol) and 2-fluoro-5-methylaniline (2.43 g, 19.3 mmol) instead of 4-fluoro-2-methylaniline, and in the same manner as in Example 1 step 1, the title compound (3.80 g, 50%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-44272be6342c4b838debe97b30601f2d |
| Source note | uspto-grants-2014_08 |