HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-fluoroaniline → HCID 71179004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-fluoroaniline | HCID 75015 | — |
| Reactant | HCID 178469627 | HCID 178469627 | — |
| Product | HCID 71179004 | HCID 71179004 | 71.2% |
Reaction Steps
Using ethyl 7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylate (2.0 g, 9.65 mmol) and 5-chloro-2-fluoroaniline (1.26 g, 8.69 mmol) instead of 4-fluoro-2-methylaniline, and in the same manner as in Example 1 step 1, the title compound (2.07 g, 64%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-f9f666ab2b394957bc0fbcff7600cbb3 |
| Source note | uspto-grants-2014_08 |