HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionic Acid → HCID 53377925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionic Acid | HCID 1032 | — |
| Reactant | HCID 71179002 | HCID 71179002 | — |
| Product | HCID 53377925 | HCID 53377925 | 87.1% |
Reaction Steps
Using 7-(2,5-difluorophenylamino)-6-[4-(4-fluorophenyl)piperidine-1-carbonyl]pyrazolo[1,5-a]pyrimidine-3-sulfonamide (0.050 g, 0.094 mmol) obtained in Example 35 step 5 and propionic acid (0.035 mL, 0.471 mmol) instead of cyclopropanecarboxylic acid, and in the same manner as in Example 1 step 6, the title compound (0.048 g, 86%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-714c74d4de75448cb30ca73ffcb1b39d |
| Source note | uspto-grants-2014_08 |