HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 71178930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 71178918 | HCID 71178918 | — |
| Product | HCID 71178930 | HCID 71178930 | 61.2% |
Reaction Steps
Using 7-(2,3-dichlorophenylamino)-6-[4-(4-fluorophenyl)piperidine-1-carbonyl]pyrazolo[1,5-a]pyrimidine-3-sulfonamide (0.050 g, 0.089 mmol) obtained in step 5 and acetic acid (0.025 mL, 0.444 mmol) instead of cyclopropanecarboxylic acid, and in the same manner as in Example 1 step 6, the title compound (0.033 g, 61%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-e2b3921f16c64ac3ba54a06a82c99c3f |
| Source note | uspto-grants-2014_08 |