HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptoethanol → HCID 43392529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptoethanol | HCID 1567 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2(3H)-Furanone, 3-bromodihydro- | HCID 95463 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 43392529 | HCID 43392529 | — |
Reaction Steps
To a solution of 2-mercapto-ethanol (2560 μmol) in THF (4 ml) were added DIEA (1.1 eq) and 3-bromo-dihydro-furan-2-one (1 eq). The reaction mixture was stirred at RT for 4 hours. The precipitate was filtered and the solvent was removed under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815873B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-709ddc184fc9442abd65bad124262a5a |
| Source note | uspto-grants-2014_08 |