HCID 58424956, compound → HCID 58424877, compound

Participants

Reaction Steps

The compound (30 mg, 0.09 mmol) prepared in step 5 was dissolved in ethanol (4 ml)/dichloromethane (2 ml), added with 10%-palladium (Pd) (6 mg) at room temperature. The resulting mixture was stirred for one day under hydrogen gas. By using celite, 10%-palladium (Pd) was removed and the filtrate was concentrated under reduced pressure. Elthyl acetate was added and the precipitate was collected by filtration to obtain the title compound (28 mg, yield: 92%, white solid).

Provenance & Evidence