HCID 58424875, compound → HCID 58424926, compound

Participants

Reaction Steps

The compound (40 mg, 0.122 mmol) prepared in step 6 was dissolved in dichloromethane/methanol (5 ml), added with 10%-palladium (Pd) (4 mg). The resulting mixture was stirred under hydrogen gas for one day at room temperature. Once the reaction was completed, the solution was filtered with celite and the filtrate was concentrated to dryness. The residue was then purified by flash column chromatography (chloroform:methanol=10:1) to obtain the title compound (40 mg, yield: 99%, white solid).

Provenance & Evidence