HCID 58424880, compound → HCID 58424853, compound

Participants

Reaction Steps

The compound (110 mg, 0.67 mmol) prepared in step 8 was dissolved in dichloromethane/methanol (10 ml), added with 10%-palladium (11 mg). The resulting mixture was stirred for one day at room temperature under hydrogen gas. Once the reaction was completed, the solution was celite-filtered and the filtrate was concentrated to dryness. The residue was then purified by flash column chromatography (chloroform:methanol=10:1) to obtain the title compound (112 mg, yield: 99%, white solid).

Provenance & Evidence