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HRID240957

反应详情

EQUATION

反应方程式

HRID 240957 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1ccc(S(=O)(=O)Cl)n1C
HCID2736899

Methyl 5-(chlorosulfonyl)-1-methyl-1H-pyrrole-2-carboxylate

C7H8ClNO4S

结构：Nc1ccc(F)c(F)c1Nc1ccc(I)cc1F
HCID59386306

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(S(=O)(=O)Nc2ccc(F)c(F)c2Nc2ccc(I)cc2F)n1C
HCID53492226

未命名化合物

PROCEDURE

实验过程

According to the general procedure B, 5,6-difluoro-N1-(2-fluoro-4-iodophenyl)benzene-1,2-diamine was reacted with methyl 5-(chlorosulfonyl)-1-methyl-1H-pyrrole-2-carboxylate to obtain the title compound. 1H NMR (300 MHz, CDCl3): δ 7.37 (dd, J=1.8 & 10.5 Hz, 1H), 7.29 (m, 2H), 7.12-6.94 (m, 4H), 5.87 (dt, J=1.8, 8.4 & 17.4 Hz, 1H), 5.56 (br s, 1H), 3.65 (s, 3H), 3.75 (s, 3H).