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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2409668Generated: October 31, 2026

3-Aminopyridine → HCID 59292880, compound

https://huagongshe.com/reaction/2409668

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-AminopyridineHCID 10009—
ReactantHCID 59292875HCID 59292875—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 59292880HCID 59292880—

Reaction Steps

The title compound was prepared in analogy to the procedure described in Step 14.1 but using 3-aminopyridine, 8-(2,6-dichloro-3,5-dimethoxy-phenyl)-2-(4-ethyl-piperazin-1-ylmethyl)-quinoxaline-5-carboxylic acid (Step 83.1) and stirring the reaction mixture for 2 days at rt. Title compound: ESI-MS: 581.0/583.2 [M+H]+; tR=3.04 min (System 1); TLC: Rf=0.33 (DCM/MeOH, 9:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08815901B2
Source datasetuspto-grants-2014_08
ORD IDord-5d1ddab206d449b895fd1b8c77f2fd41
Source noteuspto-grants-2014_08