HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-4-iodoaniline → 3-Ethyl-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-4-iodoaniline | HCID 185694 | — |
| Reactant | 1-Ethyl-3,4,5-trifluoro-2-nitrobenzene | HCID 59386371 | — |
| Product | 3-Ethyl-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline | HCID 59386347 | 60% |
Reaction Steps
2-Fluoro-4-iodoaniline (2.05 g, 10 mmol) and 1-ethyl-3,4,5-trifluoro-2-nitrobenzene (2.37 g, 10 mmol) were reacted using the condition described in example 1 (Step A) to form the title compound (2.47 g, 60%); m/z=407 [M−1]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648116B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-30304e9f4c224bdc8f8e4f62a28b217c |
| Source note | uspto-grants-2014_02 |