HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → N-(2-methoxyphenyl)-3-nitrobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| Product | N-(2-methoxyphenyl)-3-nitrobenzenesulfonamide | HCID 2834884 | 89.5% |
Reaction Steps
Using o-anisidine (1.0 ml, 8.55 mmol) and 3-nitrobenzenesulfonyl chloride (1.95 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.36 g (89.5%) of the title compound in the form of light yellow needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-df69311069264a20a142aa147b4fbb47 |
| Source note | uspto-grants-1998_03 |