Isopropylamine → HCID 86707782, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described for Intermediate K from 4-carboxy-2-methoxyphenyl boronic acid and isopropylamine. The solvent was removed and then water and EtOAc were added. The phases were separated and the aqueous one was extracted twice with EtOAc. The organic extracts were combined and dried (Na2SO4), and concentrated. The residue was triturated in acetonitrile to give the title compound. tR: 0.63 min (LC-MS 2); ESI-MS: 238.5 [M+H]+ (LC-MS 2).

Provenance & Evidence