HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-m-toluidine → HCID 86707786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-m-toluidine | HCID 67981 | — |
| Reactant | ethyl 2-bromo-5-((4-chlorophenyl)(hydroxy)methyl)-1-isopropyl-1H-imidazole-4-carboxylate | HCID 86707749 | — |
| Product | HCID 86707786 | HCID 86707786 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described for step E2 but using intermediate B and 4-fluoro-3-methylaniline. After completion, the reaction mixture was extracted with HCl and washed with a saturated NaHCO3 solution. The organic was dried (Na2SO4), filtered and concentrated. The product was used without further purification. tR: 1.37 min (LC-MS 2); ESI-MS: 508.1/510.1 [M+H]+ (LC-MS 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815926B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-020388290f6c4effbaf188832f0e2b3e |
| Source note | uspto-grants-2014_08 |