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HRID241028

反应详情

EQUATION

反应方程式

HRID 241028 的结构方程式

REACTANTS

反应物

3
结构：C[C@@H](NC(=O)OCc1ccccc1)C(=O)O
HCID70832

未命名化合物

结构：Nc1cc(Br)cnc1N
HCID691156

5-Bromopyridine-2,3-diamine

C5H6BrN3

结构：C[Si](C)(C)CCOCCl
HCID2724271

2-Chloromethyl 2-(trimethylsilyl)ethyl ether

C6H15ClOSi

PRODUCTS

生成物

1
结构：C[C@H](c1nc2cc(Br)cnc2n1COCC[Si](C)(C)C)N(COCC[Si](C)(C)C)C(=O)OCc1ccccc1
HCID68773284

未命名化合物

PROCEDURE

实验过程

Synthesized according to the method of reagent preparation 19 by using 5-bromo-2,3-diaminopyridine and N-(benzyloxycarbonyl)-D-alanine in step 1 and 2-(trimethylsilyl)ethoxymethyl chloride in step 3. MS (EI) for C28H43BrN34O4Si2: 636 (MH+).

WORKUP

后处理

  1. customSynthesized
  2. customaccording to the method of reagent preparation 19