4-(Dimethylamino)butyric acid → HCID 66605023, compound

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Reaction Steps

This was similarly prepared from 7-amino-3-(3-methoxyphenyl)-9H-carbazole-1-carboxamide and 4-(dimethylamino)butanoic acid. MS (ESI) m/z 445.26 (M+H). 1H NMR (500 MHz, MeOD) δ ppm 8.45 (1H, d, J=1.83 Hz), 8.14 (1H, d, J=1.53 Hz), 8.10 (1H, d, J=8.55 Hz), 8.05 (1H, d, J=1.83 Hz), 7.35-7.39 (3H, m), 7.29 (1H, dd, J=8.39, 1.68 Hz), 6.93 (1H, dt, J=7.55, 2.02 Hz), 3.91 (3H, s), 2.54-2.61 (2H, m), 2.50 (2H, t, J=7.32 Hz), 2.40 (6H, s), 1.91-2.02 (2H, m).

Provenance & Evidence